Combustible Dust Lab Services ISO17025 Accredited Lab
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In response to ongoing industrial / agricultural accidents related to the ignition of combustible dusts, OSHA has issued Directive #: CPL 03-00-008, Subject: Combustible Dust National Emphasis Program. The purpose of this program is to inspect facilities that generate or handle combustible dusts and make recommendations to the inspected parties that will reduce the risk of fire hazard which could result in bodily injury, loss of life and property damage. Combustible dusts are often either organic or metal dusts that are finely ground into very small particles, fibers, fines, chips, chunks, flakes, or a small mixture of these. Types of dusts include, but are not limited to: metal dust, such as aluminum and magnesium; wood dust; plastic dust; biosolids; organic dust, such as sugar, paper, soap, and dried blood; and dusts from certain textiles. Some industries that handle combustible dusts include: agriculture, chemicals, textiles, forest and furniture products, wastewater treatment, metal processing, paper products, pharmaceuticals, and recycling operations (metal, paper, and plastic). Therefore, the directive covers a wide range of materials used in many application areas across almost all the major industrial and agricultural sectors.
Combustible Dust Testing Options:
Initial Dust Characterization
The most important information determined in this stage are Percent Combustible Dust. This is the percentage of the sample that has the potential to be combustible when it is dry and fine enough to pass through a 40 mesh sieve (less than 420 µm in size). The testing includes:
- Percent through 40 Mesh Screen
- Percent Moisture Content
- Percent Combustible Material (calculated)
- Percent Combustible Dust (calculated)
Go – No Go Testing (Explosive Screening) – ASTM E1226
This is an economical and practical way to determine if the dust in the sample has the potential to be explosive. Testing consists of exposing the fine dust in the sample to low energy igniters inside the 20-Liter Siwek explosion chamber and determine the explosion over pressure. If the dust is not found to be an explosive threat, the analysis can be aborted to avoid unnecessary fees. If the sample turns out to be explosive on the screen testing, the more comprehensive analyses listed below should be conducted.
Explosion Severity (Kst, Pmax, [dP/dt]max) – ASTM E1226
This testing provides an indication of the severity of the dust explosion by determining the deflagration parameters. The larger the value of Kst, the more severe the explosion is. For this test, the dust is suspended and ignited in the Siwek chamber and the maximum pressureand the rate of pressure rise are measured.
Minimum Explosion Concentration (MEC) – ASTME1515
MEC is the minimum concentration for explosivity of a combustible dust cloud. It is determined by suspending the dust in the Siwek Chamber.
Minimum Ignition Energy (MIE) – ASTM E2019
MIE is the electrical energy discharged from a capacitor, just sufficient to produce the ignition of the most ignitable mixture of air and dust. It is determined by suspending the dust in a Hartmann Lucite explosion chamber.
Minimum Ignition Temperature Test (MIT) – ASTM E1491 (dust cloud)ASTM E2021 (dust layer)
This test method covers the minimum temperature at which a dust cloud will autoignite when exposed to air and heated in a furnace at atmospheric pressure. It is determined by introducing the dust into a BAM oven. As an alternative, the minimum temperature of self-ignition of dust layer can be measured using a hot plate set-up.
Class II Testing
This level of testing involves a number of parameters that determine if the sampled dust is considered a Class II hazardous material. Class II locations are defined as locations with combustible dust having Ignition Sensitivity (I.S.) greater than or equal to 0.2 or Explosion Severity (E.S.) greater than or equal to 0.5. I.S. is calculated from MIT, MIE, and MEC for the sample normalized to Pittsburg coal dust, whereas E.S. is calculated from Pmax and[dP/dt]max for the sample, also normalized to Pittsburg coal dust.
Resistivity Testing (for metal dust in particular)
FREE Combustible Dust Poster for Environmental Professionals
The resistivity testing is particularly important for metal dust. The electrical nature of the dust is one criteria to determine if it is necessary to take special precaution with regard to electrical insulation of the equipment operating in a location with Class II dust.
Combustibility Screening Test (VDI 2263 2.1.1)
A dust is considered explosible if there is a flame propagation after igniting the dust/air mixture resulting in a pressure rise in a closed vessel. This test is conducted in the Hartmann 1.2 Liter Vessel. The sample is tested over a range of concentrations and is submitted to a continuous induction spark as an ignition source.
Limiting Oxygen Concentration (LOC - ASTM E2931)
This test method is designed to determine the limiting oxygen concentration of a combustible dust dispersed in a mixture of air with an inert/nonflammable gas. The testing is performed in the 20-L Siwek chamber.
Layer Ignition Temperature (LIT – ASTM E2021)
This test method determines the hot-surface ignition temperature of dust layers, that is, measuring the minimum temperature at which a dust layer will self-heat. The test consists of a dust layer heated on a hot plate.
EPA 1030/CFR § 49.173 –Ignitability of Solids
This method is suitable for the determination of the ignitability of solids. Material is formed into an unbroken strip or powder train. An ignition source is applied to one end of the test material to determine whether combustion will propagate within a specified time period. If propagation occurs, material is submitted to a burning rate test. In the burning rate test, burning time is measured over a distance and a burning rate is determined. Materials that do not ignite or propagate combustion do not require further testing.
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